Mariner 4
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The Mariner 4 mission, the second of two Mars flyby attempts in 1964 by NASA, was one of the great early successes of the agency, and indeed the Space Age, returning the very first photos of another planet from deep space.
Using a new all metal shroud, the spacecraft lifted off without any problems and was successfully boosted towards Mars by the Agena D upper stage. A single midcourse correction on Dec. 5, 1964 ensured that the spacecraft would fly between 5,000 and 6000 miles (8,000 and 9,660 kilometers) from the Martian surface.
On one of the scientific instruments, the plasma probe, there was a component failure making its readings unintelligible, although due to a better telemetry rate, some data was received between January and May 1965. Additionally a Geiger tube, one of the two sensors in the ionization chamber experiment, failed and stopped returning data in March 1965.
Approximately 40 minutes prior to closest approach (which was at 01:00:57 UT July 15, 1965 at a range of 6,118 miles (9,846 kilometers), the TV camera began taking the first of 21 images (plus 22 lines of a 22nd image) through red and green filters.
About 1.25 hours after the encounter, Mariner 4 dipped behind the right hand side of Mars (as viewed from Earth) in an occultation experiment in order to refract its radio signals through the Martian atmosphere. Data indicated that surface pressure was quite low, i.e., future Mars landers would have to be equipped with retro-rocket engines in addition to parachutes.
The images as well as the occultation experiment fundamentally transformed the scientific view of the Red Planet, providing hard data where speculation had previously dominated. The probe detected daytime surface temperatures at minus 148 degrees Fahrenheit (minus 100 degrees Celsius). A very weak radiation belt, about 0.1% of that of Earth’s, was also detected.
The day after the closest encounter, Mariner 4 began transmitting its photos back to Earth. The images clearly showed Mars to be an ancient Moon-like body with widespread cratering, thus incontrovertibly quashing any expectations of lost civilizations on the planet. Given the thin atmosphere, scientists believed that it was unlikely that Mars harbored any life.
NASA maintained contact with the spacecraft until Oct. 1, 1965 when the probe was 192 million miles (309 million kilometers) from Earth. Two years later, in October 1967, the spacecraft was reactivated for attitude control tests in support of the Mariner 5 mission to Venus that used a similar spacecraft bus. Contact was maintained until Dec. 31, 1967, over three years after launch.
Source
Siddiqi, Asif A. Beyond Earth: A Chronicle of Deep Space Exploration, 1958-2016. NASA History Program Office, 2018.