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Link to original content: https://pubmed.ncbi.nlm.nih.gov/27739098
Synthesis of stable isotope labeled D9 -Mabuterol, D9 -Bambuterol, and D9 -Cimbuterol - PubMed Skip to main page content
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. 2016 Nov;59(13):546-551.
doi: 10.1002/jlcr.3446. Epub 2016 Oct 13.

Synthesis of stable isotope labeled D9 -Mabuterol, D9 -Bambuterol, and D9 -Cimbuterol

Yahui Tu  1 , Jiaqi Zhong  1 , Haoran Wang  1 , Jie Pan  1 , Zhongjie Xu  1 , Weicheng Yang  1 , Yong Luo  1
Affiliations

Synthesis of stable isotope labeled D9 -Mabuterol, D9 -Bambuterol, and D9 -Cimbuterol

Yahui Tu et al. J Labelled Comp Radiopharm. 2016 Nov.

Abstract

Three stable and simple synthetic routes of labeled D9 -Mabuterol, D9 -Bambuterol, and D9 -Cimbuterol were described with 98.5%, 99.7%, and 98.4% isotopic abundance and good purity. These structures and isotope-abundance were confirmed according to 1 H NMR and liquid chromatography-tandem mass spectrometry.

Keywords: internal standards; isotope labeling; synthesis; β-agonist.

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